Small tube furnaces used in laboratories perform well in most scenarios, with advantages such as high-precision temperature control, flexible atmosphere control, and compact design. However, they have limitations such as limited sample processing capacity and high maintenance costs, and need to be selected based on experimental needs. The following is a detailed analysis of its advantages and disadvantages:
advantage
High precision temperature control
Small tube furnaces are usually equipped with PID intelligent temperature control systems, with a temperature control accuracy of ± 1 ℃. Some models support multi-stage programmed heating (such as 30 stages), which can accurately control the heating temperature and ensure the accuracy and repeatability of experiments. This is particularly important for experiments that require precise temperature control, such as the synthesis of nanomaterials and the study of metal phase transitions.
Flexible atmosphere control
Inert gases (such as nitrogen and argon), reducing gases (such as hydrogen), or oxidizing gases can be introduced, supporting a vacuum environment (with a vacuum degree of up to 10 ⁻ Pa) to meet the reaction conditions of different materials. For example, when growing graphene by CVD, methane and hydrogen gas need to be introduced at 1000 ℃, and oxygen pollution should be strictly avoided.
Compact design and space utilization
The length of the furnace tube is usually 300-1200mm, with a diameter of 20-100mm and a small footprint (such as 0.2m ²), making it suitable for laboratory desktop operations. Some models, such as vertical tube furnaces, adopt a vertical design for easy sample loading, unloading, and observation, especially suitable for gravity sensitive scenarios such as crystal growth and deposition experiments in the vertical direction.
Uniform heating and energy-saving design
Heating elements (such as silicon molybdenum rods and resistance wires) are designed to surround the furnace to ensure temperature uniformity (within ± 5 ℃) and avoid local overheating. Adopting ceramic fiber material and double-layer shell structure, the temperature rise and fall speed is fast, the energy consumption is low, and the external temperature can be lowered to room temperature, reducing heat loss.
Modularity and Scalability
The furnace body, temperature control system, and gas path system are detachable for easy cleaning or replacement of components (such as heating elements). Some models offer single temperature zone, dual temperature zone, or triple temperature zone options, supporting gradient temperature control, suitable for experiments that require different temperature zones (such as material diffusion research).
Safety and operational convenience
Equipped with multiple safety devices such as over temperature protection, thermocouple protection, and leakage protection to ensure safe operation. Some models adopt a quick opening flange design, which supports rapid cooling and meets the requirements of material rapid cooling and heating experiments. User friendly interface, supports RS-485 serial port or software remote control, and can achieve linkage of single or multiple devices.