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Can a desktop mini tube stove be ventilated with gas?

Time:2025-11-04 Click:0
  

The desktop mini tube furnace can pass gas, and its gas control function is one of its core advantages, which is reflected in the following aspects:

1. Gas type compatibility
Inert gas: Supports nitrogen (N ₂), argon (Ar), etc., used to prevent material oxidation or decomposition (such as high-temperature sintering of ceramics, synthesis of nanomaterials).
Reductive gases: can be introduced with hydrogen (H ₂), carbon monoxide (CO), etc., to participate in chemical reactions (such as metal surface carburizing, catalyst reduction).
Oxidative gas: Some models support oxygen (O ₂) or air, suitable for oxidation experiments such as metal oxidation and catalyst calcination.
Mixed gas: Through a dual inlet design, the ratio of inert/reducing gases can be adjusted (such as argon+hydrogen mixed atmosphere).

2. Gas control accuracy
Flow regulation: Equipped with a mass flow controller (MFC) or a float flowmeter to accurately control gas flow (such as 0-500sccm), ensuring reaction stability.
Airtight design: using double ring sealing flanges, silicone sealing rings or quick opening flanges to prevent gas leakage (vacuum degree can reach 10 ⁻ Pa).
Pressure monitoring: Some models are integrated with mechanical pressure gauges, which display real-time furnace air pressure (range -0.1 to 0.15 MPa) to avoid the risk of excessive pressure.

3. Typical application scenarios
Chemical Vapor Deposition (CVD): A precursor gas (such as SiH ₄, NH3) is introduced at high temperature to deposit a thin film (such as silicon nitride, graphene) on a substrate.
Nanomaterial synthesis: Pyrolysis of precursors in an inert atmosphere to synthesize high-purity nanoparticles (such as TiO ₂ SiC)。
Metal heat treatment: Annealing and quenching in hydrogen or argon gas to improve the mechanical properties of metals (such as stainless steel powder metallurgy).
Catalyst preparation: Calcination of alumina support in nitrogen and loading of active components (such as Pt/Al ₂ O3 automotive exhaust catalyst).
Semiconductor process: Gallium nitride thin films are grown by MOCVD in a mixed atmosphere of ammonia and trimethyl gallium.

4. Operation and safety design
Program temperature control: supports multi-stage program temperature control (such as 30 stages), can preset gas inlet time and temperature curve, and achieve automated experiments.
Security protection:
Overtemperature alarm: Automatically shuts off when the temperature exceeds the set value.
Pressure interlock: Automatically exhausts when the air pressure is too high to prevent the furnace tube from bursting.
Furnace temperature protection: Do not open the furnace door when the furnace temperature is ≥ 300 ℃ to avoid burns.
Convenient maintenance: Modular design facilitates the replacement of gas path components (such as flow meters and sealing rings), reducing maintenance costs.

5. Actual cases
Ceramic sintering: Vacuum sintering alumina ceramics in an argon atmosphere at 1600 ℃, with high density, suitable for electronic packaging substrates.
Metal powder metallurgy: Stainless steel powder is reduced and sintered in hydrogen at 1400 ℃, with low porosity, and used for 3D printing of metal parts.
Preparation of catalyst support: Calcination of γ – Al ₂ O3 in a nitrogen atmosphere at 800 ℃, with a large specific surface area, used for automobile exhaust purification.

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