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Advantages of industrial multi temperature zone rotary furnace

Time:2025-11-10 Click:0
  

The industrial multi temperature zone rotary furnace exhibits significant advantages in heat treatment, drying, sintering and other processes through unique structural design and technological integration, especially suitable for the production of high-precision and high value-added materials. The following is a detailed analysis of its core advantages:

1. Independent control of multiple temperature zones: the key to precise process implementation
Accurate control of temperature gradient
Technical implementation: The furnace body is divided into multiple independent temperature zones along the axial direction (usually 3-12), each equipped with independent heating elements (such as resistance wires, induction coils) and temperature sensors (such as thermocouples, infrared thermometers), and temperature closed-loop control is achieved through PLC or DCS system.
Advantage:
Complex process adaptation: It can simultaneously meet the temperature requirements of different materials or different stages of the same material. For example, in the sintering of positive electrode materials for lithium batteries, the front temperature zone (200-400 ℃) is used for dehydration, the middle temperature zone (600-800 ℃) is used for crystal transformation, and the back temperature zone (900-1000 ℃) is used for densification to avoid overburning or undercorning caused by a single temperature.
Thermal stress control: Reduce internal thermal stress of materials by gradient heating/cooling to prevent cracking or deformation. For example, in the sintering of ceramic materials, the multi temperature zone design reduces the heating rate from the traditional single temperature zone of 10 ℃/min to 3 ℃/min, resulting in a decrease in residual stress.
Dynamic process optimization
Technical implementation: The temperature in the temperature zone can be adjusted in real time, combined with the furnace rotation speed (usually 0.5-5rpm) and material residence time (controlled by speed or feed rate), to achieve dynamic matching of process parameters.
Advantage:
Adapt to material changes: When there are differences between material batches (such as particle size and moisture content), process deviations can be compensated for by adjusting the temperature zone. For example, in the drying of pharmaceutical intermediates, if a batch of materials is detected to have a high moisture content, the corresponding temperature range can be automatically increased by 5-10 ℃ to ensure consistent drying.
Energy saving and consumption reduction: Dynamically close non essential temperature zones according to the process stage to reduce energy waste. For example, in the drying of semiconductor silicon powder, only the first three temperature zones are opened during the dehydration stage, and all temperature zones are opened during the sintering stage, resulting in a reduction in comprehensive energy consumption.

2. Efficient heat transfer and mixing: the core of improving process efficiency
Three dimensional hybrid enhanced heat transfer
Technical implementation: The furnace body is installed at a tilt angle of 1-5 °, and combined with rotational motion, the material generates complex motion trajectories in the axial, radial, and circumferential directions (such as “rolling+sliding+shearing”), forming a three-dimensional mixing effect.
Advantage:
Heat transfer coefficient improvement: The mixing effect increases the contact frequency between the material and the heating surface, and the heat transfer coefficient is 3-5 times higher than that of a static furnace. For example, in metal powder sintering, the heat transfer coefficient of a multi zone rotary furnace reaches 80-120W/(m ² · K), while that of a static furnace is only 20-40W/(m ² · K).
Temperature uniformity optimization: Three dimensional mixing reduces the internal temperature gradient of materials, avoiding local overheating or undercooling. For example, in the drying of lithium battery materials, the standard deviation of material temperature in multi temperature zone rotary furnaces is less than 5 ℃, while in static furnaces it reaches 5-8 ℃.
Short process technology implementation
Technical implementation: Through synergistic optimization of mixing and heat transfer, multi-step processes (such as drying, preheating, and sintering) can be completed within a single device, reducing material transfer and equipment switching time.
Advantage:
Shortening production cycle: For example, in the production of ceramic capacitor dielectric materials, the multi temperature zone rotary furnace reduces the traditional process (drying furnace → preheating furnace → sintering furnace) from 72 hours to 24 hours, increasing production capacity.
Pollution risk reduction: Reduce the time that materials are exposed to the external environment and lower the risk of introducing impurities. For example, in semiconductor material processing, the cleanliness of multi zone rotary furnaces can reach Class 100 (ISO 5), which is an order of magnitude higher than traditional multi equipment series processes.

3. Vacuum and Atmosphere Control: Ensuring the Preparation of High end Materials
Adaptability to vacuum environment
Technical implementation: Equipped with a vacuum system (such as rotary vane pump+Roots pump+molecular pump), it can achieve high vacuum (≤ 10 ⁻ ² Pa) or low vacuum (10 ³ -10 ⁵ Pa) environment, combined with sealing structures (such as labyrinth seal, magnetic fluid seal) to prevent air leakage.
Advantage:
Oxidation sensitive material treatment: isolate O ₂/N ₂ under vacuum to prevent oxidation of metals (such as Ti, Al) or organic compounds (such as active pharmaceutical ingredients). For example, in the sintering of titanium alloy powder, vacuum reduces the oxygen content and increases the tensile strength of the material.
Low temperature process implementation: Vacuum reduces the boiling point of materials (such as the boiling point of water dropping to 7 ℃ at 100Pa), which can quickly dry/sinter at low temperatures and reduce thermal damage. For example, in the drying of bioactive substances, vacuum reduces the temperature from 120 ℃ to 60 ℃, resulting in an increase in activity retention rate.
Atmosphere protection flexibility
Technical implementation: Inert gases (such as N ₂, Ar) or reducing gases (such as H ₂ CO), Accurately control gas flow rate (0.1-100L/min) and ratio (such as H ₂/N ₂=4:96) in conjunction with a quality flow meter.
Advantage:
Reductive atmosphere treatment: In the reduction sintering of metal powders, H ₂ atmosphere can remove surface oxides and improve material purity. For example, in tungsten powder reduction, a multi temperature zone rotary furnace reduces oxygen content and achieves higher purity under an H ₂ atmosphere.
Carbonization/Nitriding Process Support: In the production of hard alloys, the introduction of CH ₄ or N ₂ can achieve carbonization or nitriding reactions, forming WC or TiN coatings. For example, in tool coating treatment, the multi temperature zone rotary furnace increases the hardness of the coating under N ₂ atmosphere, which is higher than traditional processes.

4. Modularization and Intelligence: Adapting to the Trend of Flexible Production
Modular design scalability
Technical implementation: The furnace body adopts a segmented structure, and each temperature zone can be independently disassembled or replaced, supporting rapid transformation to adapt to different material or process requirements.
Advantage:
Equipment reuse rate improvement: For example, the same multi zone rotary furnace can be used for lithium battery material drying, ceramic sintering, or metal powder reduction by replacing the temperature zone module, which increases the return on investment of the equipment.
Flexible adjustment of production capacity: By increasing or decreasing the number of temperature zones (such as expanding from 6 temperature zones to 10 temperature zones), it is possible to quickly match changes in production capacity demand and avoid equipment idle or overloaded.
Intelligent control integration
Technical implementation: Integrated PLC/DCS system, HMI operation interface, and SCADA data acquisition platform, supporting real-time monitoring of process parameters, historical data traceability, and remote diagnosis.
Advantage:
Process stability improvement: AI algorithms are used to automatically optimize temperature, rotation speed, and gas flow rate in the temperature zone, reducing human operational errors. For example, in the drying of pharmaceutical intermediates, intelligent control improves the difference between product batches (CPK value) and meets GMP standards.
Predictive maintenance: By monitoring the operating status of equipment through sensors (such as heating element resistance, bearing temperature), early warning of fault risks and reducing unplanned downtime. For example, in a certain production line, intelligent systems improve the overall efficiency of equipment.

5. Typical application scenarios and data support
Production of lithium battery materials
Scenario: Drying and sintering of positive electrode materials (such as NCM, LFP).
Advantages: The multi temperature zone design reduces moisture content, increases sintering density, and saves energy compared to traditional processes.
Semiconductor Material Processing
Scenario: Drying of silicon powder and sintering of silicon carbide (SiC).
Advantages: The vacuum environment results in high purity of silicon powder, better density of SiC sintering, and shortened investment payback period for single line equipment.
Preparation of pharmaceutical intermediates
Scenario: Drying and crystallization of highly active pharmaceutical ingredients (APIs).
Advantages: Three dimensional mixing reduces the standard deviation of crystal particle size distribution (D50), minimizes solvent residue, and meets FDA requirements.

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